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Tar vs Soot testing: Soluble separation method

Bear Kaufmann finished another run on the GEK test and datalogging rig and posted the results here: http://gekgasifier.pbworks.com/Instrumented-Walnut-Shell-Run-082409. This wiki page has a large collection of graphs and other data assemblies from the run. Bear is very clever. Someday he’ll get a Phd in all this. In the interim, we get to ponder his bi-weekly posting of dissertation worthy test runs and data visualizations. Thank you Bear.

The main issue he was/is trying to resolve in this test is how to measure tar. The usual “simplified tar testing method” with the greyscale seems very open to mixing the tar and soot signal on the filter paper. both tar and soot are “black”. Filtering before the sample tends to reduce both of them indiscriminately. So we’re trying instead to take the sample without any prefiltering, and dissolve the tar out of the sample with a solvent, and then measure the color/hue/greyscale of the liquid.

Does anyone here have any experience with this type of soluble tar testing method? Or otherwise have any input on the accuracy or import of the attempted tar-soot separation method?

In the pix above, and in the more detailed report linked above, you will see that [...]